Design and optimization of photonic crystal fiber for liquid sensing applications

Photonic Sensors, Jun 2016

This paper proposes a hexagonal photonic crystal fiber (H-PCF) structure with high relative sensitivity for liquid sensing; in which both core and cladding are microstructures. Numerical investigation is carried out by employing the full vectorial finite element method (FEM). The analysis has been done in four stages of the proposed structure. The investigation shows that the proposed structure achieves higher relative sensitivity by increasing the diameter of the innermost ring air holes in the cladding. Moreover, placing a single channel instead of using a group of tiny channels increases the relative sensitivity effectively. Investigating the effects of different parameters, the optimized structure shows significantly higher relative sensitivity with a low confinement loss.

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Design and optimization of photonic crystal fiber for liquid sensing applications

Citation: Md. Faizul Huq ARIF, Kawsar AHMED, Sayed ASADUZZAMAN, and Md. Abul Kalam AZAD, “Design and Optimization of Photonic Crystal Fiber for Liquid Sensing Applications,” Photonic Sensors Design and Optimization of Photonic Crystal Fiber for Liquid Sensing Applications Corresponding author: Kawsar AHMED 2 Md. Faizul Huq ARIF 1 2 Kawsar AHMED 1 2 Sayed ASADUZZAMAN 1 2 Md. Abul Kalam AZAD 0 2 0 Department of Material and Metallurgical Engineering (MME), Bangladesh University of Engineering and Technology 1 Department of Information and Communication Technology (ICT), Mawlana Bhashani Science and Technology 2 University (BUET) , Dhaka-1000 , Bangladesh This paper proposes a hexagonal photonic crystal fiber (H-PCF) structure with high relative sensitivity for liquid sensing; in which both core and cladding are microstructures. Numerical investigation is carried out by employing the full vectorial finite element method (FEM). The analysis has been done in four stages of the proposed structure. The investigation shows that the proposed structure achieves higher relative sensitivity by increasing the diameter of the innermost ring air holes in the cladding. Moreover, placing a single channel instead of using a group of tiny channels increases the relative sensitivity effectively. Investigating the effects of different parameters, the optimized structure shows significantly higher relative sensitivity with a low confinement loss. Photonic crystal fiber (PCF); liquid sensor; microstructure core; sensitivity; confinement loss 1. Introduction The field of fiber optics is no longer limited into telecommunication and medical science only; it has been developing in an incredible pace with large dimensions of applications. Fiber optic technologies have made a revolutionary change after the invention of photonic crystal fiber (PCF). PCF is a new class of optical fiber which is one of the recent inventions in the field of fiber optics. PCF can be used as a transmission media as well as optical functional devices. In contrast to the conventional optical fiber, PCFs have additional design features, such as air-hole diameter, pitch size, and number of rings, which offer to overcome many limitations of conventional fiber. Due to the well-known advantages, such as enhanced design freedom, low cost, short-time detection, small size, robustness, and high sensitivity and flexibility PCFs have received considerable attention in developing optodevices and sensors. Photonic crystal fibers (PCFs) have been attracted a great deal of attention for its incredible performance and large variety of applications. PCF can be used as filters [ 1 ], switches [ 2, 3 ], electro-optical modulators [ 4, 5 ], polarization converters [ 6 ], sensors [ 7‒17 ], etc. PCF based sensors are smart applications in fiber optic technology which have been investigating and developing since last decade. A wide range of sensing applications of PCF are available, such as temperature sensors [ 7 ], refractive index (R.I) sensors [ 8 ], chemical sensors [ 9 ], mechanical sensors [ 10 ], pressure sensors [ 11 ], gas sensors [ 12,13 ], stress sensors [14], pH sensors [ 15 ], liquid sensors [ 16 ], biosensors [ 17 ], and so on. An ideal candidate of optical sensors is index guiding PCF. The sensing mechanism of index guiding PCF is evanescent interaction between the optical field and the analyte to be sensed. The evanescent field based PCF sensors have been developing rapidly for chemical and biomedical applications due to their attractive features. Highly sensitive chemical (liquid and gas) sensors are playing an important role in the industrial processes [ 18 ] especially for detecting toxic and flammable chemicals (e.g., toxic gasses or liquids) to overcome the safety issues. So it has become one of the key challenges to enhance the performance of liquid and gas sensors. In recent years, researchers are keeping much interest on the development of photonic crystal fiber (PCF) based sensors for environmental and safety monitoring [ 19, 20 ] issues. Photonic crystal fiber based liquid and gas sensors through the evanescent field show excellent performance in terms of sensitivity, because core of the PCF directly interacts with the material to be analyzed. PCF technologies allow for the accurate tuning of fiber through changing the air hole shape, size, and their position. A wide variety of PCF based sensing techniques have been reported by changing different geometric parameters of the PCF to gain sensitivity at a maximum and confinement loss at a minimum satisfactory level in liquid and gas sensing applications. J. Park et al. [ 21 ] enhanced relative sensitivity for chemical sensing, using a hexagonal PCF with a hollow high indexed ring defect. In the hollow core PCF, the direct interaction between light and the analyte in the hollow channel is higher than the index-guided PCFs. Recently, the idea of filling core or cladding holes with various liquids or gases has been attracted much to the researchers. Cordeiro et al. [ 22 ] proposed a microstructure core PCF infiltrated with liquid analyte which enhanced the evanescent field. This concept introduced the sensing potentiality with infiltrated microstructure core. PCF of microstructure core offers to sense low indexed material because of the highly interaction of evanescent fields with the analyst to be sensed. A large number of published papers investigated and enhanced the performance of PCF based gas and liquid sensors with microstructure core [ 23‒28 ]. In recent study, higher sensitivity and lower confinement loss of microstructure core PCF for liquid sensing have been attempted by using octagonal cladding structure [ 24, 25 ]. Reference [25] suggested 5-ring octagonal PCF for higher sensitivity and lower confinement loss; but in practical manufacturing octagonal structure requires extra more capillaries than the hexagonal structure. Keeping large number of capillaries will make high cost to fabricate. In this point of view, liquid sensing using a single infiltrated channel may also reduce the complexity of the core. To the best of our knowledge, no studies have been done in analyzing the sensitivity performance of PCF with a liquid filled core of a single channel. In this research work, we have proposed and optimized simple evanescent hexagonal structure of PCF (H-PCF) with microstructure core and cladding for liquid sensing, which shows high relative sensitivity as well as low confinement loss. We have also explained the effect of single infiltrated channel replacing the microstructure core by proposing another structure of PCF, which achieved more enhancements of relative sensitivity and simplicity in design. We have not used any defect around the hollow core; though one of the previous articles [ 21 ] enhanced relative sensitivity by using a ring defect around the core. The relative sensitivity and confinement loss against different liquids (water, ethanol, and benzyne) have been investigated and compared. Although we have chosen water, ethanol, and benzyne as the targeted chemical species for characterization of our structures but these structures and the mechanism can be applied for all fluids and gases based on the absorption line of the targeted sample. 2. Design principle Figure 1 shows the transverse cross sectional view of the four stages of our proposed PCF structure. The proposed PCF contains only four layers of air holes in the cladding. The distance between center and center of two adjacent air holes (pitch distance) has been denoted by . The diameters of air holes in the innermost ring, second ring, third ring, and outermost ring are d1, d2, d3, and d4, respectively. In PCF1, the diameter of all air holes is equal, where d1=d2=d3=d4. In our numerical investigation, we found that the outermost ring holes diameter has greater impact on the confinement loss, and then we have come into PCF2. In PCF2, d1=d2=d3<d4. Another result of our numerical investigation shows that larger diameter of the innermost ring holes enhances the sensitivity and we have turned into PCF3. In PCF3, optimized values of air holes diameter have been kept as d2=d3<d1=d4. However, we have turned into PCF4 and achieved higher sensitivity by replacing the group of tiny holes with a single hollow core filled with same analyte to be detected. The hollow core area is same as the area covered by supplementary tiny holes. In the PCF1, PCF2, and PCF3, the core is designed with some tiny holes in circular form which are filled with various liquid samples: water, ethanol, and benzyne for this study. These supplementary core holes are arranged with the hole to hole pitch distance denoted by a. Figure 2 visualizes the enlarged view of core of PCF1, PCF2, PCF3, and the replacement of hollow channel instead of using a group of tiny channels in PCF4. Diameter of the hollow channel is D2=1.70 m, which is same as the diameter of the region of supplementary holes in the core (D1=D2). Figure 3 shows the computational region of the proposed PCF3 and PCF4, which is divided into homogeneous triangular pieces forming a mesh. Each of the PCFs has two orthogonal sides of the computational region which are assigned with two artificial boundary conditions: perfect electric conductor (PEC) and perfect magnetic conductor (PMC). Perfectly matched layer (PML) is used as a boundary condition. Thickness of the PML is fixed to 10% of the radius of the proposed PCFs for efficient calculation of confinement loss [ 29 ]. d4 d3 d2 d1 d4 d3 d2 d1 PCF3 PCF4 (c) (d) Fig. 1 Transverse cross sectional view of (a) PCF1, (b) PCF2,  (c) PCF3, and (d) PCF4.             a a a D1 D2   (a) (b) Fig. 2 Enlarged view of core region of (a) PCF1, PCF2, and PCF3 and (b) PCF4. 3. Principles of operation PCFs act as a waveguide, and in this wave guide, d4 d3 d2 d1 d4 d3 d2 d1 PCF1 (a) PCF2 (b) d1=d2=d3=d4   d2=d3<d1=d4 d1=d2=d3<d4  d1=d2<d3=d4  and the targeted analyte and light interact with each other. We have analyzed the evanescent field distribution of the proposed PCFs. Using the finite element method (FEM), the properties of propagating mode of the proposed PCFs is numerically investigated. We have considered circular perfectly matched layer (PML) as a boundary condition. The cross sections of the proposed PCFs are divided into homogeneous triangular subspaces using mesh analysis shown in Fig. 3. The liquid filled air holes’ region is then divided into many sub-domains which are either triangular or quadrilateral in shape. Using FEM, Maxwell’s equations are solved by accounting neighboring subspaces. As the wave propagates through z direction, the modal analysis has been performed in the x-y plane of the PCF structure. The following vectorial wave equation can be derived from the Maxwell’s equation [ 30 ]. PMC PMC Y (a) Y (b) PEC PML PML X PEC Fig. 3 FEM meshes and boundary conditions for computation of (a) PCF3 and (b) PCF4.   (S1  E)  k02n2SE  0 (1) where S represents the PML matrix of 3×3 and S1 is the inverse of S matrix. The symbol E denotes the electric field vector, n is the refractive index of the domain, K0 is the wave number in free space, and  is the operating wavelength. The propagating constant  is represented by the following equation.   neff K0 (2) Due to the finite number of air holes in the cladding part, there may cause leakage of light. The leakage of light from core to exterior materials results in confinement loss (dB/m) which can be obtained from the imaginary part of neff by using the following equation [ 24 ]. Lc  8.868  K0 Im[neff ]dB/m . (3) However, this leakage of light energy can be omitted by using an infinite number of air holes. But in practical, the number of air holes is finite. The relative sensitivity coefficient measures the interaction between the light and the analyte to be sensed. This interaction is measured through the absorption coefficient at a particular wavelength. According to the Beer-Lambert law, light is attenuated by the intensity of absorption of evanescent wave [ 31 ] I( )  I0( ) exp[r mlc ] (4) The absorbance of the sample to be detected is defined by the following equation [ 27 ]:  I  A  lg  I0   r mlc (5) where I and I0 are the input and output intensities, respectively, and c is the concentration of absorbing material. The length of the channel is l. The function of absorption coefficient is  m( ) , and r is the relative sensitivity coefficient, which can be defined by the following equation [ 22 ] r  nnerff f (6) where nr refers to the refractive index of the sample to be sensed, and neff is the effective index of the guided mode. f is the fraction of total power located in the core, and it is also known as a power distribution function [ 28 ] by using Poynting’s theorem which can be expressed as the following equation: f  holes Re(ExH y  EyH x )dxdy total Re(ExH y  EyH x )dxdy where Ex and Hx are transverse electric field and (7) 1.42 1.41 x 1.40 e d in 1.39 e v ti fec 1.38 f E 1.37 1.36 1.35 PCF1, n=1.330, X-polarization PCF2, n=1.330, X-polarization PCF3, n=1.330, X-polarization 1.340.6 0.7 0.8 0.9 1.0 1.1 1.2 1.3 1.4 1.5 1.6 Wavelength (m) Fig. 4 Effective index curves of the fundamental mode  for the X-polarization with =2.4 m, d=0.45 m. PCF1: d1=d2=d3=d4=1.9 m; PCF2: d1=d2=d3=1.9 m and d4= 2.15 m; PCF3: d2=d3=1.9 m and d1=d4=2.15 m. 4. Results and discussion This section describes the numerical analysis of propagation characteristics in fundamental mode and some higher order modes of the proposed PCFs. Three liquid analytes, water, ethanol, and benzyne, have been selected for filling the supplementary core holes. Here, it has been considered X-polarization of fundamental mode for this investigation. The initial analysis has been performed by assuming the geometric parameters of PCF1: d1=d2=d3=d4=1.9 m; PCF2: d1=d2=d3=1.9 m and d4=2.15 m; PCF3: d2=d3=1.9 m and d1=d4=2.15 m. The supplementary holes pitch ratio is d/a=0.70. The center-to-center air holes distance is =2.4 m at the cladding, which has been kept fixed for all of the proposed PCFs. The simulation has been performed at a wide range of wavelength from 0.6 m to 1.6 m. The simulation process has been down using COMSOL Multiphysics 4.2 by selecting a fine mode of mesh size. The convergence error seems very low of proposed PCFs about 3.55×10−5% and 3.50× 10−5 % for PCF3 and PCF4, respectively. 30 25 ) % t(y 20 itii v s n eS 15 30 25 )( % y iitv 20 it se n S 15 10 30 25 )( % y iitv 20 it se n S 15 magnetic field respectively; Ey and Hx are longitudinal electric field and magnetic field respectively. Using FEM the mode field pattern and effective index are obtained. During the simulation, we have considered the material dispersion of silica background using the Sellmeier equation [ 32 ]. Initially, Fig. 4 shows the effective index profile of PCF1, PCF2, and PCF3. It is clear from Fig. 4 that the effective indices decrease linearly with an increase in wavelength. It can be evidently seen that the PCF1 shows higher effective index values among the first three proposed PCFs. PCF1, d1/=d2/=d3/=d4/=0.83, n=1.366 10 PCF2, d1/=d2/=d3/=0.83, d4/=0.93, n=1.366 PCF3, d2/=d3/=0.83, d1/=d4/=0.93, n=1.366 0.6 0.7 0.8 0.9 1W.0avele1n.g1th (m1.)2 1.3 1.4 1.5 1.6 (c) Fig. 5 Comparison of the relative sensitivity of PCF1, PCF2, and PCF3 for (a) water, (b) ethanol, and (c) benzyne, where =2.4 m, d=0.45 m. PCF1: d1=d2=d3=d4=1.9 m; PCF2: d1=d2=d3=1.9 m, and d4=2.15 m; PCF3: d2=d3=1.9 m, and d1=d4=2.15 m. 10 PCF1, d1/=d2/=d3/=d4/=0.83, n=1.33 PCF2, d1/=d2/=d3/=0.83, d4/=0.93, n=1.33 PCF3, d2/=d3/=0.83, d1/=d4/=0.93, n=1.33 0.6 0.7 0.8 0.9 1.0 1.1 1.2 1.3 1.4 1.5 1.6 Wavelength (m) (a)   PCF1, d1/=d2/=d3/=d4/=0.83, n=1.354 PCF2, d1/=d2/=d3/=0.83, d4/=0.93, n=1.354 PCF3, d2/=d3/=0.83, d1/=d4/=0.93, n=1.354 0.6 0.7 0.8 0.9 1W.0avele1n.g1th (m1.)2 1.3 1.4 1.5 1.6 (b) Figure 5 presents the relative sensitivity curves of PCF1, PCF2, and PCF3 for the three analytes as a function of wavelength. There is no significant change in sensitivity for PCF1 and PCF2 in all wavelengths. Therefore, no significant impacts on sensitivity have been observed with increasing diameters of outer rings holes. However, the relative sensitivity of PCF3 is greatly enhanced. At the wavelength =1.33 m, for water, ethanol, and benzyne, the calculated sensitivity of PCF3 is 30%, 32.5%, and 33.67%, respectively and the confinement loss is 3.25×10−10 dB/m, 2.95×10−10 dB/m, and 2.31×10−10 dB/m, respectively. The reason behind the enhanced sensitivity of PCF3 is that the increment of the inner ring holes diameter leads them closer to the core area and the fraction of evanescent field penetrates to the holes increase and relative sensitivity of the PCF3 increases consequently. It is also clear that higher index material shows higher relative sensitivity. Figure 6 illustrates the relative sensitivity performance of PCF3 varying the diameter (d) of the supplementary holes in the core region. According to this inquiry, the sensitivity increases with the increment of the diameter of supplementary holes. From Fig. 6, we have found the highest relative sensitivity when d=0.55 m. For this value of the supplementary holes diameter, PCF3 shows relative sensitivity 48.50% and 47.78%, and confinement loss 1.28×10−10 dB/m and 5.37×10−11 dB/m for ethanol and water, respectively, at the wavelength =1.33 m. To achieve much more relative sensitivity, we have proposed PCF4 replacing a single hollow channel instead of using supplementary tiny holes. In PCF4, the diameter of the hollow channel is D2=1.70 m. Figure 7 depicts the comparative performance of sensitivity of the last two proposed PCFs: PCF3 and PCF4 for all types of analytes used in this study. According to Fig. 7, PCF4 shows great enhancement of relative sensitivity. At the 50 45 40 )35 % (y30 ti v itis25 n e S20 15 10 5 50 45 40 35 ) (%30 y t itiv25 i s n eS20 15 10 5 60 50 ) % (y40 ittii v sen30 S 20 wavelength =1.33 m, PCF4 exhibits the relative sensitivity 50%, 55.83%, and 59.07%, confinement loss 4.25×10−10 dB/m, 8.72×10−10 dB/m, and 2.56×10−10 dB/m for water, ethanol, and benzyne, respectively. d1/=d4/=0.93, d2/=d3/=0.83, n=1.354, d=0.45 m d1/=d4/=0.93, d2/=d3/=0.83, n=1.354, d=0.50 m d1/=d4/=0.93, d2/=d3/=0.83, n=1.354, d=0.55 m 0.6 0.7 0.8 0.9 1W.0avele1n.g1th (m1.)2 1.3 1.4 1.5 1.6 (a)   d1/=d4/=0.93, d2/=d3/=0.83, n=1.33, d=0.45 m d1/=d4/=0.93, d2/=d3/=0.83, n=1.33, d=0.50 m d1/=d4/=0.93, d2/=d3/=0.83, n=1.33, d=0.55 m 0.6 0.7 0.8 0.9 1.0 1.1 1.2 1.3 1.4 1.5 1.6 Wavelength (m) (b) Fig. 6 Comparison of relative sensitivity of PCF3 as a function of operating wavelength for (a) ethanol (b) water; where d=0.45 m, d=0.50 m, d=0.55 m, and rest of the parameters are fixed as before. 70 PCF3, n=1.330 PCF3, n=1.354 PCF3, n=1.366 PCF4, n=1.330 10 PCF4, n=1.354 PCF4, n=1.366 Fig. 70.R6ela0t.7ive 0s.8ensi0t.9ivity1W.0avveelre1ns.gu1ths(wm1.)2avel1e.3ngth1.4 for1.5PCF13.6 a nd PCF4 with =2.4 µm, d=0.55m, D2=1.70 m, d2=d3=1.9 m, and d1=d4=2.15 m. Figure 8 presents the confinement loss curves of PCF3 and PCF4. With the investigation of Fig. 8, it can be seen that PCF4 exhibits better performance in terms of confinement loss for all types of analytes used in this study. Therefore, it can be said that the light mode is more confined in the core region for the proposed PCF4 compared with the first three proposed PCF structures. This may be linked to the fact that the electromagnetic interaction between the propagated light and analyte is higher which causes an increase in relative sensitivity. In addition, from Fig. 8, it can be found that lower confinement losses are achieved with higher indexed liquids. According to the overall discussion, PCF4 shows higher sensitivity and lower confinement loss than PCF3. 109 /) m B d (s so1010 lt n e m e n if n o C1011 PCF3, n=1.330 PCF3, n=1.354 PCF3, n=1.366 PCF4, n=1.330 PCF4, n=1.354 PCF4, n=1.366 10120.6 0.7 0.8 0.9 1.0 1.1 1.2 1.3 1.4 1.5 1.6 Wavelength (m) Fig. 8 Confinement loss versus wavelength for PCF3 a  nd PCF4 with =2.4 µm, d=0.55 µm, D2=1.70 µm, d2=d3=1.9 m, and d1= d4=2.15 m. In order to support the numerical results reported in the figures, the electric field distribution of the proposed PCF3 and PCF4 has been illustrated in Fig. 9, where the operating wavelength is set to =1.33 m and the core holes are filled with ethanol. It can be clearly seen that the fundamental mode of our optimized PCFs (PCF3 and PCF4) is tightly confined in the core region. From the overall discussion, we have found that our designed structures show better performance in relative sensitivity with more design simplicity than the prior structures [ 24, 25 ] for liquid sensing. Table 1 shows the comparative performance analysis Structural shape description Octagonal shape: 3 rings Octagonal shape: 5 rings Hexagonal shape: 4 rings Hexagonal shape: 4 rings between prior PCFs and proposed PCFs for liquid sensing at the wavelength =1.33 m. Tables 2 and 3 represent the sensitivity dependency on diameters and global parameters variations, respectively. Although, diameters are varied after fabrication but it has no global effects on result of the proposed structure. Through the experimental point of view, the fabrication feasibility of the proposed PCFs is an important part. It seems that the fabrication process of the micro cored region may not be easy. However, due to the technological advancement, the fabrication of our recommended PCFs is possible. Micro core must be filled with the analyte without damaging the fiber’s integrity. Now, several techniques are available for filling the PCF holes with analytes. Huang et al. [ 33 ] proposed a unique method for selectively filling the all cladding holes as well as micro core holes. The fabrication of PCF with liquid filled core or cladding can be accomplished with the same method [ 34, 35 ]. Now, applying the sol-gel technique [36] any kind of complexity of fabrication of microstructure optical fiber can be removed. In this regard, our proposed PCF structures can be fabricated with the currently available nanotechnology. Selective filling technique [ 37 ] can be used for fill the analytes (gas or liquids) at the core. 20 10 5. Conclusions In this study, the enhancement of the performance of the PCF based liquid sensor has been done by our recommended two structures of PCF, which are based on microstructure core and hollow core, and infiltrated with the liquid to be sensed. All of the proposed structures with microstructure core and liquid core have better guiding capability and the manufacturing of this type of structure is possible with the current nanofabrication techniques [ 34−38 ]. Our proposed PCF provided higher relative sensitivity with tighter confinement of optical field than the prior PCF structures. Therefore, our proposed PCFs can successfully overcome the critical trade-off between confinement loss and sensitivity, and it is assumed that our proposed structures of PCF offer great potentiality for toxic chemical and gas detection in industrial safety purposes. 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Md. Faizul Huq Arif, Kawsar Ahmed, Sayed Asaduzzaman, Md. Abul Kalam Azad. Design and optimization of photonic crystal fiber for liquid sensing applications, Photonic Sensors, 2016, 279-288, DOI: 10.1007/s13320-016-0323-y